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Gas Chromatography and Mass Spectrometry for Thujone, Pinocamphone, and Fenchone A previously described procedure was used (14) , which was extended for the analysis of pinocamphone and fenchone. The sample preparation was accomplished using liquid–liquid extraction with 1,1,2-trichloro-1,2,2-trifluoroethane after the method of Rapp et al. (15) .

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Gas Chromatography-Mass SpectrometryA microanalytical technique coining mass spectrometry and gas chromatography for the qualitative as well as quantitative determinations of compounds. Random Alloion A process involving chance used in therapeutic trials or other research endeavor for alloing experimental subjects, human or animal

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The added benefit of simultaneous olfactometry (O) and chemical analysis (e.g., by gas chromatography-mass spectrometry (GC-MS)) allows for characterization of trace amounts of compounds with detection limits below that of the mass detector (i.e., 2-isobutyl-3-methoxypyrazine, a “green bell pepper” aroma with detection threshold less than 0

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CyanatesOrganic salts of cyanic acid containing the -OCN radical. Carbon-Nitrogen LyasesEnzymes that alyze the cleavage of a carbon-nitrogen bond by means other than hydrolysis or oxidation.Subclasses are the AMMONIA-LYASES, the AMIDINE-LYASES, the amine-lyases, and other carbon-nitrogen lyases. EC 4.3.

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Volatile compounds were analysed using a headspace solid-phase microextraction (SPME) method coupled with gas chromatography-mass spectrometer and flame ionization detector (GC-MS/FID), as reported by Lu et al. . Liquid juice or wine samples were centrifuged, and the pH was adjusted to 2.5 by 1 M HCl, and a 5 mL sample was sealed in a 20-mL

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The added benefit of simultaneous olfactometry (O) and chemical analysis (e.g., by gas chromatography-mass spectrometry (GC-MS)) allows for characterization of trace amounts of compounds with detection limits below that of the mass detector (i.e., 2-isobutyl-3-methoxypyrazine, a “green bell pepper” aroma with detection threshold less than 0

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